7-[[6-O-(6-脱氧-alpha-L-甘露糖基)-beta-D-吡喃葡萄糖基]氧基]-3,5-二羟基-2-(3-羟基-4-甲氧基苯基)-4H-苯并吡喃-4-酮合成路线 (共 3 条)
反应条件
1: With dihydrogen peroxide; sodium hydroxide in water T=0°C; 48 h; 2: With acetic acid in water T=0°C; pH=6; 3: With Na2S2O5 in water 2 h; Reflux;
参考文献
Lewin, Guy; MacIuk, Alexandre; Moncomble, Aurelien; Cornard, Jean-Paul
Journal of Natural Products, 2013 , vol. 76, # 1 p. 8 - 12
反应条件
1: With dihydrogen peroxide; sodium hydroxide in water T=0°C; Algar-Flynn-Olyamada (AFO) reaction; 48 h; 2: With acetic acid in water T=0°C; pH=6; 24 h; 3: With Na2S2O5 in water 2 h; Reflux;
参考文献
Lewin, Guy; MacIuk, Alexandre; Thoret, Sylviane; Aubert, Genevieve; Dubois, Joelle; Cresteil, Thierry
Journal of Natural Products, 2010 , vol. 73, # 4 p. 702 - 706
反应条件
hydrogenchloride; water T=55°C; 1.5 h;
参考文献
Lewin, Guy; MacIuk, Alexandre; Thoret, Sylviane; Aubert, Genevieve; Dubois, Joelle; Cresteil, Thierry
Journal of Natural Products, 2010 , vol. 73, # 4 p. 702 - 706