2,3,4,6-四邻乙酰基-alpha-d-氟代半乳糖氯化物合成路线 (共 12 条)
反应条件
bismuth(III) chloride; methyltrichloromonosilane in dichloromethane Ambient temperature;
参考文献
Montero, Jean-Louis; Winum, Jean-Yves; Leydet, Alain; Kamal, Mehrnaz; Pavia, Andre A.; Roque, Jean-Pierre
Carbohydrate Research, 1997 , vol. 297, # 2 p. 175 - 180
反应条件
2,4,6-trichloro-1,3,5-triazine; 1,8-diazabicyclo[5.4.0]undec-7-ene; N,N-dimethyl-formamide in 1,2-dichloro-ethane T=60°C; 2 h;
参考文献
Chang, Chih-Wei; Chang, Shih-Sheng; Chao, Chin-Sheng; Mong, Kwok-Kong T.
Tetrahedron Letters, 2009 , vol. 50, # 31 p. 4536 - 4540
反应条件
dichloromethoxy methane; zinc(II) chloride in chloroform 22 h;
参考文献
Jansson, Karl; Noori, Ghazi; Magnusson, Goeran
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3181 - 3185
反应条件
2,6-di-tert-butyl-4-methylpyridine; boron trichloride in dichloromethane T=0°C;
参考文献
Perdomo, Guillermo R.; Krepinsky, Jiri J.
Tetrahedron Letters, 1987 , vol. 28, # 46 p. 5595 - 5598
反应条件
aluminum oxide in acetonitrile T=20°C; 4.5 h;
参考文献
Tiwari, Pallavi; Misra, Anup Kumar
Carbohydrate Research, 2006 , vol. 341, # 3 p. 339 - 350
反应条件
aluminium trichloride in dichloromethane T=50°C; 2 h;
参考文献
Rajanikanth, B.; Seshadri, R.
Tetrahedron Letters, 1987 , vol. 28, # 20 p. 2295 - 2296
反应条件
in chloroform; ethyl acetate; Petroleum ether
参考文献
Ciba-Geigy Corporation
Patent: US5218097 A1, 1993 ;
反应条件
zirconium tetrachloride; ethanethiolic acid in dichloromethane 96 h; Ambient temperature;
参考文献
Defaye, Jacques; Driguez, Hugues; Ohleyer, Eric; Orgeret, Catherine; Viet, Catherine
Carbohydrate Research, 1984 , vol. 130, p. 317 - 321
反应条件
hydrogenchloride; acetyl chloride T=-70°C;
参考文献
Korytnyk; Mills
Journal of the Chemical Society, 1959 , p. 636,644
反应条件
hydrogenchloride; acetyl chloride T=-70°C;
参考文献
Korytnyk; Mills
Journal of the Chemical Society, 1959 , p. 636,644