in tetrahydrofuran under Ar; PhC2H added to soln. of Ru-Pt complex (room temp., stirring);soln. at -78°C warmed to room temp.; stirred (ca. 25°C, 3-12 h); aliquot taken; solvent freed; residue studied by NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 593-594, p. 465 - 478
in tetrahydrofuran under Ar; PhC2Ph added to soln. of Ru-Pt complex (room temp., stirring); soln. at -78°C warmed to room temp.; stirred (ca. 25°C, 3-12 h); aliquot taken; solvent freed; residue studied by NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 593-594, p. 465 - 478
in tetrahydrofuran (argon); NMR tube: addn. of the ligand to the Pt complex in THF at -78°C, slight warming for dissoln., recooling to -80°C; NMR monitoring;
参考文献
Journal of the Chemical Society - Dalton Transactions, , # 6 p. 1039 - 1043
