in chloroform-d1 byproducts: MeP(O)(PPh)2; under N2; phosphine (5-100 equiv.) added to soln. of Pd complex in CDCl3at 25°C; 24 h; not isolated; monitored by (1)H and (31)P NMR spectra;
参考文献
Stockland Jr., Robert A.; Levine, Adam M.; Giovine, Matthew T.; Guzei, Ilia A.; Cannistra, Joseph C.
Organometallics, 2004 , vol. 23, # 4 p. 647 - 656
in chloroform-d1 byproducts: MeP(O)(PPh)2; under N2; phosphine (5-100 equiv.) added to soln. of Pd complex in CDCl3at 25°C; 24 h; not isolated; monitored by (1)H and (31)P NMR spectra;
参考文献
Stockland Jr., Robert A.; Levine, Adam M.; Giovine, Matthew T.; Guzei, Ilia A.; Cannistra, Joseph C.
Organometallics, 2004 , vol. 23, # 4 p. 647 - 656
in benzene byproducts: acetylacetone, triphenylphosphine oxide; fast (5 min) and quantitative reaction after adding stoichiometric amt. of water; products not isolated, reaction monitoring by NMR;
参考文献
Russian Journal of General Chemistry, , vol. 67, # 1 p. 53 - 57
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, # 10 p. 2144 - 2149
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 2347 - 2352
