1(1R,2R)-(+)-1-苯基亚丙基环氧合成路线 (共 69 条)
反应条件
sodium ethanolate in methanol T=0 - 20°C;
参考文献
Besse; Renard; Veschambre
Tetrahedron Asymmetry, 1994 , vol. 5, # 7 p. 1249 - 1268
反应条件
molecular sieve; 2,6-dichloropyridine-N-oxide; [Ru(II)(D4-Por*)(CO)] in benzene T=20°C; 24 h; Title compound not separated from byproducts;
参考文献
Chemical Communications, , # 23 p. 2906 - 2907
反应条件
sodium hydroxide in dichloromethane; water T=38°C; 48 h;
参考文献
Kavanagh, Sarah A.; Connon, Stephen J.
Tetrahedron Asymmetry, 2008 , vol. 19, # 12 p. 1414 - 1417
反应条件
sodium hydroxide in dichloromethane; water T=38°C; 48 h;
参考文献
Kavanagh, Sarah A.; Connon, Stephen J.
Tetrahedron Asymmetry, 2008 , vol. 19, # 12 p. 1414 - 1417
反应条件
sodium hydroxide in dichloromethane; water T=38°C; 48 h;
参考文献
Kavanagh, Sarah A.; Connon, Stephen J.
Tetrahedron Asymmetry, 2008 , vol. 19, # 12 p. 1414 - 1417
反应条件
(R,R)-chromium-salen; oxygen in acetonitrile T=0°C; Yield given;
参考文献
Bousquet, Claudine; Gilheany, Declan G.
Tetrahedron Letters, 1995 , vol. 36, # 42 p. 7739 - 7742
反应条件
4-(tert-butyl)pyridine; Clorox bleach; tetradecyl benzyl dimethyl ammonium chloride; chiral manganese-porphyrin complex 6 in dichloromethane T=20°C; 4 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 56, # 18 p. 5253 - 5254
反应条件
sodium hydride in 1,4-dioxane; N,N-dimethyl-formamide 6 h; Heating;
参考文献
Belvisi, Laura; Gennari, Cesare; Poli, Giovanni; Scolastico, Carlo; Salom, Barbara; Vassallo, Marco
Tetrahedron, 1992 , vol. 48, # 19 p. 3945 - 3960
反应条件
(R,R)-[Cr(salen)] hexafluoroantimonate; 4 A molecular sieve; tert-butyl alcohol in various solvent(s) T=0°C; 36 h; Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 1 p. 84 - 87
反应条件
sodium hydroxide in dichloromethane; water 18 h; Heating;
参考文献
Rosenberger, Michael; Jackson, William; Saucy, Gabriel
Helvetica Chimica Acta, 1980 , vol. 63, # 6 p. 1665 - 1674