N-(2-羟乙基)十二烷基酰胺合成路线 （共 14 条）
反应条件
Novozym.(R). 435 in 1,4-dioxane 0.0833333 h; Microwave irradiationEnzymatic reaction; chemoselective reaction;
参考文献
Kidwai, Mazaahir; Poddar, Roona; Mothsra, Poonam
Beilstein Journal of Organic Chemistry, 2009 , vol. 5, art. no. 10
反应条件
Novozym.(R). 435 in 1,4-dioxane 0.0833333 h; Microwave irradiationEnzymatic reaction; chemoselective reaction;
参考文献
Kidwai, Mazaahir; Poddar, Roona; Mothsra, Poonam
Beilstein Journal of Organic Chemistry, 2009 , vol. 5, art. no. 10
反应条件
triethylamine in dichloromethane T=-10 - 20°C;
参考文献
Gur'eva; Budanova; Sebyakin
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 2 p. 173 - 177
参考文献
Journal of the American Chemical Society, , vol. 59, p. 111
US2236530 , ;
反应条件
1: thionyl chloride / 1 h / 20 °C 2: triethylamine / dichloromethane / 0.25 h / 20 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 3 p. 851 - 864
反应条件
in dichloromethane T=20°C; Cooling with ice;
参考文献
Archiv der Pharmazie, , vol. 342, # 1 p. 34 - 40
反应条件
1: With sodium hydroxide; sodium hypochlorite; 4-acetylamino 2,2,6,6-tetramethylpiperidin-N-oxyl; potassium bromide in water; toluene T=31 - 38°C; pH=6.9 - 8.9; 5 - 6 h; 2: With hydrogenchloride in tetrahydrofuran; water; toluene pH=2.2; Product distribution / selectivity;
参考文献
Conopco, Inc., d/b/a UNILEVER
Patent: US2007/299269 A1, 2007 ;
Location in patent: Page/Page column 6; 7 ;
反应条件
triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=20°C; 24 h; Inert atmosphere;
参考文献
Xu, Quancai; Li, Zhengning; Chen, Huiying
Chinese Journal of Chemistry, 2011 , vol. 29, # 5 p. 925 - 932
反应条件
1: With sodium hydroxide; sodium hypochlorite; 4-acetylamino 2,2,6,6-tetramethylpiperidin-N-oxyl; potassium bromide in water; toluene T=31 - 38°C; pH=6.9 - 8.9; 5 - 6 h; 2: With hydrogenchloride in tetrahydrofuran; water; toluene pH=2.2; Product distribution / selectivity;
参考文献
Conopco, Inc., d/b/a UNILEVER
Patent: US2007/299269 A1, 2007 ;
Location in patent: Page/Page column 6; 7 ;
