2-甲氧基-3-甲基环戊-2-烯-1-酮合成路线 (共 20 条)
反应条件
(i) iBu2AlH, Et2O, hexane, (ii) aq. H2SO4, dioxane; Multistep reaction;
参考文献
Helvetica Chimica Acta, , vol. 58, # 2 p. 564 - 584
反应条件
5,15,10,20-tetraphenylporphyrin in dichloromethane
Ambient temperatureIrradiation;
参考文献
Kwon, Byoung-Mog; Foote, Christopher S.
Journal of Organic Chemistry, 1989 , vol. 54, # 16 p. 3878 - 3882
反应条件
oxygen; rose bengal
T=-20°C; 2.5 h; Irradiation; Title compound not separated from byproducts;
参考文献
Kwon, Byoung-Mog; Foote, Christopher S.
Journal of Organic Chemistry, 1989 , vol. 54, # 16 p. 3878 - 3882
反应条件
oxygen; rose bengal
T=-20°C; 2.5 h; Irradiationother solvents, other temperature; Product distribution;
参考文献
Kwon, Byoung-Mog; Foote, Christopher S.
Journal of Organic Chemistry, 1989 , vol. 54, # 16 p. 3878 - 3882
反应条件
oxygen; rose bengal
T=-35°C; 3 h; Irradiation; Product distribution;
参考文献
Kwon, Byoung-Mog; Foote, Christopher S.
Journal of Organic Chemistry, 1989 , vol. 54, # 16 p. 3878 - 3882
反应条件
1: sodium hydride / diethyl ether; paraffin / Heating
2: tetrabutylammonium hydrogen sulfate, aq. sodium hydroxide / CH2Cl2 / 0.33 h
View Scheme
参考文献
Arnarp, Jan; Enzell, Curt; Petersson, Kurt; Pettersson, Tore
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 10 p. 839 - 854
反应条件
5,15,10,20-tetraphenylporphyrin in dichloromethane
Ambient temperatureIrradiation;
参考文献
Kwon, Byoung-Mog; Foote, Christopher S.
Journal of Organic Chemistry, 1989 , vol. 54, # 16 p. 3878 - 3882
反应条件
oxygen; rose bengal
T=-20°C; 2.5 h; Irradiation; Title compound not separated from byproducts;
参考文献
Kwon, Byoung-Mog; Foote, Christopher S.
Journal of Organic Chemistry, 1989 , vol. 54, # 16 p. 3878 - 3882
反应条件
oxygen; rose bengal
T=-20°C; 2.5 h; Irradiationother solvents, other temperature; Product distribution;
参考文献
Kwon, Byoung-Mog; Foote, Christopher S.
Journal of Organic Chemistry, 1989 , vol. 54, # 16 p. 3878 - 3882
反应条件
oxygen; rose bengal
T=-35°C; 3 h; Irradiation; Product distribution;
参考文献
Kwon, Byoung-Mog; Foote, Christopher S.
Journal of Organic Chemistry, 1989 , vol. 54, # 16 p. 3878 - 3882