N-[2-(3,4-二甲氧基苯基)乙基]-4-甲基苯磺酰胺合成路线 （共 8 条）
反应条件
triethylamine in tetrahydrofuran 12 h;
参考文献
McKillop, Alexander; Davies, Huw M. L.; Taylor, Edward C.
Synthetic Communications, 1986 , vol. 16, # 3 p. 267 - 282
反应条件
1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C 2: pyridine; phosphorus tribromide / dichloromethane / 1 h / 0 - 20 °C / |Inert atmosphere 3: ammonia / ethanol; water / 4 h / 20 °C 4: triethylamine / acetonitrile / 4 h / 20 °C View Scheme
参考文献
Kiruthika, Selvarangam E.; Perumal, Paramasivan Thirumalai
Organic Letters, 2014 , vol. 16, # 2 p. 484 - 487
反应条件
1: pyridine; phosphorus tribromide / dichloromethane / 1 h / 0 - 20 °C / |Inert atmosphere 2: ammonia / ethanol; water / 4 h / 20 °C 3: triethylamine / acetonitrile / 4 h / 20 °C View Scheme
参考文献
Kiruthika, Selvarangam E.; Perumal, Paramasivan Thirumalai
Organic Letters, 2014 , vol. 16, # 2 p. 484 - 487
反应条件
1: ammonia / ethanol; water / 4 h / 20 °C 2: triethylamine / acetonitrile / 4 h / 20 °C View Scheme
参考文献
Kiruthika, Selvarangam E.; Perumal, Paramasivan Thirumalai
Organic Letters, 2014 , vol. 16, # 2 p. 484 - 487
反应条件
1: LiAlH4 2: NaOH / CH2Cl2 View Scheme
参考文献
Silveira, Claudio C.; Bernardi, Carmem R.; Braga, Antonio L.; Kaufman, Teodoro S.
Tetrahedron Letters, 1999 , vol. 40, # 27 p. 4969 - 4972
反应条件
1: NH4OAc; AcOH 2: LiAlH4 3: NaOH / CH2Cl2 View Scheme
参考文献
Silveira, Claudio C.; Bernardi, Carmem R.; Braga, Antonio L.; Kaufman, Teodoro S.
Tetrahedron Letters, 1999 , vol. 40, # 27 p. 4969 - 4972
反应条件
1: 61 percent / SnCl4 / CH2Cl2 / -78 deg C -> r.t. 2: 95 percent / REDAL / toluene View Scheme
参考文献
Silveira, Claudio C.; Bernardi, Carmem R.; Braga, Antonio L.; Kaufman, Teodoro S.
Tetrahedron Letters, 1999 , vol. 40, # 27 p. 4969 - 4972
反应条件
potassium carbonate; acetone
anschliessend mit wss.NaOH;
参考文献
Proctor; Thomson
Journal of the Chemical Society, 1957 , p. 2312
