甲基 2,3-O-异亚丙基-alpha-L-吡喃鼠李糖苷合成路线 (共 11 条)
反应条件
sulfuric acid; copper(II) sulfate 12 h;
参考文献
Van Summeren, Ruben P.; Feringa, Ben L.; Minnaard, Adriaan J.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 14 p. 2524 - 2533
反应条件
boron trifluoride diethyl etherate in acetone T=0 - 20°C; 12.5 h;
参考文献
Capozzi; Ciampi; Delogu; Menichetti; Nativi
Journal of Organic Chemistry, 2001 , vol. 66, # 26 p. 8787 - 8792
反应条件
toluene-4-sulfonic acid 2 h;
参考文献
Priebe; Skibicki; Neamati; Achmatowicz; Grynkiewicz; Szechner
Polish Journal of Chemistry, 1999 , vol. 73, # 7 p. 1143 - 1152
反应条件
methanol; sodium amalgam
参考文献
Muskat
Journal of the American Chemical Society, 1934 , vol. 56, p. 2653,2655
Full Text Show Details
Levene; Compton
Journal of the American Chemical Society, 1935 , vol. 57, p. 2306,2307
Journal of Biological Chemistry, 1936 , vol. 114, p. 9,19
反应条件
tri-n-butyl-tin hydride Yields of byproduct given;
参考文献
Pozsgay, Vince; Neszmelyi, Andras
Carbohydrate Research, 1980 , vol. 85, p. 143 - 150
参考文献
Levene; Compton
Journal of the American Chemical Society, 1935 , vol. 57, p. 2306,2307
Journal of Biological Chemistry, 1936 , vol. 114, p. 9,19
Full Text Show Details
Levene; Muskat
Journal of Biological Chemistry, 1934 , vol. 106, p. 761,768, 769
反应条件
in benzene 72 h; Irradiation;
参考文献
Yamashita, Mitsuji; Long, Pham T.; Shibata, Masayuki; Inokawa, Saburo
Carbohydrate Research, 1980 , vol. 84, p. 35 - 42
反应条件
1: 3.5percent HCl / 4 h / Heating 2: copper (II) sulphate, Drierite / dimethylformamide View Scheme
参考文献
Batavyal, Lakshmi; Roy, Nirmolendu
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 5 p. 499 - 500
反应条件
copper(II) sulfate 24 h; Heating;
参考文献
MacMillan, John B.; Guang, Xiong-Zhou; Skepper, Colin K.; Molinski, Tadeusz F.
Journal of Organic Chemistry, 2008 , vol. 73, # 10 p. 3699 - 3706
反应条件
camphor-10-sulfonic acid; acetyl chloride 1.) reflux, 21 h, 2.) acetone, 18 h; Yield givenMultistep reaction;
参考文献
Davis, Benjamin G.; Nash, Robert J.; Watson, Alison A.; Smith, Colin; Fleet, George W. J.
Tetrahedron, 1999 , vol. 55, # 14 p. 4501 - 4520