2,4,5,6-四氯嘧啶合成路线 (共 22 条)
反应条件
copper in N,N-dimethyl-formamide T=150°C;
参考文献
Mack, Arthur G.; Suschitzky, Hans; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1682 - 1687
反应条件
copper; benzoyl chloride in N,N-dimethyl-formamide T=150°C; 0.5 h;
参考文献
Mack, Arthur G.; Suschitzky, Hans; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1682 - 1687
反应条件
isopropyl-benzene; copper in N,N-dimethyl-formamide T=150°C; 1 h; Further byproducts given;
参考文献
Mack, Arthur G.; Suschitzky, Hans; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1682 - 1687
反应条件
copper in N,N-dimethyl-formamide T=150°C; 20 h;
参考文献
Mack, Arthur G.; Suschitzky, Hans; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1682 - 1687
反应条件
1: 39 percent / potassium carbonate / acetone / 2 h / Heating 2: 39 percent / tetrahydrofuran; ethanol / 6 h / Irradiation 3: 40 percent / 46 h / Irradiation View Scheme
参考文献
Mack, Arthur G.; Suschitzky, Hans; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1682 - 1687
反应条件
copper in N,N-dimethyl-formamide T=150°C; 20 h;
参考文献
Mack, Arthur G.; Suschitzky, Hans; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1682 - 1687
反应条件
in diethyl ether 28 h; Irradiationfurther solvents;
参考文献
Bratt, Jack; Iddon, Brian; Mack, Arthur G.; Suschitzky, Hans; Taylor, Jack A.; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 648 - 656
反应条件
1: 4 percent / copper bronze / dimethylformamide / 150 °C 2: 22 percent Chromat. / copper bronze / dimethylformamide / 20 h / 150 °C View Scheme
参考文献
Mack, Arthur G.; Suschitzky, Hans; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1682 - 1687
反应条件
1: copper bronze / dimethylformamide / 150 °C 2: 22 percent Chromat. / copper bronze / dimethylformamide / 20 h / 150 °C View Scheme
参考文献
Mack, Arthur G.; Suschitzky, Hans; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1682 - 1687
反应条件
1: 1 percent / p-xylene, benzoyl chloride / dimethylformamide / 23 h / Heating 2: 22 percent Chromat. / copper bronze / dimethylformamide / 20 h / 150 °C View Scheme
参考文献
Mack, Arthur G.; Suschitzky, Hans; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1682 - 1687