{IrH(acetone)[2,6-(tBu2PO)2C6H3]}{BF4} in chlorobenzene-d5 T=20°C; 0.3 h; Inert atmosphere;
参考文献
Khalimon, Andrey Y.; Piers, Warren E.; Blackwell, James M.; Michalak, David J.; Parvez, Masood
Journal of the American Chemical Society, 2012 , vol. 134, # 23 p. 9601 - 9604
[Ph3S][tBu2CarbCO2B(C6F5)3] in dichloromethane-d2 T=20°C; 0.25 h; UV-irradiation;
参考文献
Khalimon, Andrey Y.; Piers, Warren E.; Blackwell, James M.; Michalak, David J.; Parvez, Masood
Journal of the American Chemical Society, 2012 , vol. 134, # 23 p. 9601 - 9604
1: 4-carboxymethyl cyclohexane With triethylamine; isobutyl chloroformate in tetrahydrofuran T=-30 - -20°C; 0.5 h; 2: ethyl acetate With lithium diisopropyl amide in tetrahydrofuran T=-70 - -65°C; 3: With hydrogenchloride in tetrahydrofuran; water
参考文献
SCHERING CORPORATION; PHARMACOPEIA, INC.
Patent: WO2004/22559 A1, 2004 ;
Location in patent: Page 32 ;
WO 2004/022559 A1
