(E)-3,7-二甲基-2,6-辛二烯醛合成路线 （共 128 条）
反应条件
1: With methyl-diethoxy-silane; Rh<(S,S)-Phebox>(OAc)2(aq) in toluene T=30°C; 1 h; 2: With potassium fluoride; tetrabutyl ammonium fluoride in tetrahydrofuran; methanol; toluene Further stages.;
参考文献
Kanazawa, Yoshinori; Nishiyama, Hisao
Synlett, 2006 , # 19 p. 3343 - 3345
反应条件
in chloroform 0.25 h; Ambient temperature; Yield given;
参考文献
Arbones, Cesar; Sanchez, Francisco J.; Marco, Maria-Pilar; Camps, Francisco; Messeguer, Angel
Heterocycles, 1990 , vol. 31, # 1 p. 67 - 78
反应条件
manganese(IV) oxide in hexane
T=0°C; 6 h;
参考文献
Tsuboi, Sadao; Ishii, Naomi; Sakai, Takashi; Tari, Isao; Utaka, Masanori
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 7 p. 1888 - 1893
反应条件
sodium hydroxide; dipotassium peroxodisulfate; nickel sulphate in dichloromethane; water
24 h; Ambient temperature; Yields of byproduct given;
参考文献
Yamazaki, Shigekazu; Yamazaki, Yasuyuki
Chemistry Letters, 1989 , p. 1361 - 1364
反应条件
hydrogenchloride; aluminum isopropoxide in ethyl acetate; benzene
参考文献
NIKKEN CHEMICALS CO., LTD.
Patent: US2002/198411 A1, 2002 ;
反应条件
ammonium cerium(IV) nitrate in methanol; water
T=20°C; Oxidation; elimination; 0.166667 h;
参考文献
Nair, Vijay; Nair, Latha G.; Balagopal, Lakshmi; Rajan, Roshini
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1999 , vol. 38, # 11 p. 1234 - 1236
反应条件
tert.-butylhydroperoxide; 4 A molecular sieve; Yb(Oi-Pr)3 in dichloromethane
T=0°C; 24 h; also with La(Oi-Pr)3, Ce(Oi-Pr)3, Sm(Oi-Pr)3;
参考文献
Lebrun, Alain; Namy, Jean-Louis; Kagan, Henri B.
Tetrahedron Letters, 1991 , vol. 32, # 21 p. 2355 - 2358
反应条件
iodobenzene; β-cyclodextrin; potassium bromide in water; acetone
T=20°C; 12 h;
参考文献
Narender; Somi Reddy; Srilakshmi Krishnaveni; Surendra; Nageswar; Rama Rao
Synthetic Communications, 2006 , vol. 36, # 10 p. 1463 - 1470
反应条件
water; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide
T=20°C; 0.75 h;
参考文献
Wu, Yikang; Huang, Jia-Hui; Shen, Xin; Hu, Qi; Tang, Chao-Jun; Li, Liang
Organic Letters, 2002 , vol. 4, # 13 p. 2141 - 2144
反应条件
β-cyclodextrin; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in water; acetone
T=20°C; 1.5 h;
参考文献
Narender; Reddy, M. Somi; Kumar, V. Pavan; Nageswar; Rao, K. Rama
Tetrahedron Letters, 2005 , vol. 46, # 12 p. 1971 - 1973
