3,7-二甲基辛-7-烯醛合成路线 （共 5 条）
反应条件
polystyrene-supported 5-hydroxy-2-iodoxybenzoic acid in dichloromethane T=20°C; 0.5 h;
参考文献
Sorg; Mengel; Jung; Rademann
Angewandte Chemie - International Edition, 2001 , vol. 40, # 23 p. 4395 - 4397
反应条件
nitroacetic acid ethyl ester; triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran room temperature for 2 h, refluxed for 2 h;
参考文献
Mitsunobu, Oyo; Yoshida, Naoyuki
Tetrahedron Letters, 1981 , vol. 22, # 24 p. 2295 - 2296
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride; ethyl acrylate in benzene Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bulliard, M.; Balme, G.; Monteiro, N.; Gore, J.
Bulletin de la Societe Chimique de France, 1991 , p. 222 - 231
反应条件
1: 71 percent / HNO3, Ac2O / 0.5 h / 0 °C 2: tributyltinhydride, AIBN, ethylacrylate / benzene / Heating View Scheme
参考文献
Bulliard, M.; Balme, G.; Monteiro, N.; Gore, J.
Bulletin de la Societe Chimique de France, 1991 , p. 222 - 231
反应条件
T=90°C; P=1 Torr; bei der Destillation;
参考文献
Carroll et al.
Journal of the Chemical Society, 1950 , p. 3457
