顺-3,7-二甲基-2,6-辛二烯-1-醇乙酸酯合成路线 (共 54 条)
反应条件
samarium diiodide; isopropyl alcohol; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tabuchi, Takanori; Inanaga, Junji; Yamaguchi, Masaru
Tetrahedron Letters, 1986 , vol. 27, # 5 p. 601 - 602
反应条件
NaY-Zeolite in hexane T=20°C; 6 h;
参考文献
Yu, Wei; Bian, Fengling; Gao, Yuan; Yang, Li; Liu, Zhong-Li
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 1-2 p. 59 - 62
反应条件
zeolite NaY in hexane T=70°C; 12 h;
参考文献
Tsangarakis, Constantinos; Stratakis, Manolis
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 9 p. 1280 - 1284
反应条件
sodium hydride; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran
T=65°C; 36 h; Yield given. Yields of byproduct given;
参考文献
Cuvigny, Therese; Julia, Marc; Rolando, C.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 395 - 414
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
6 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Petrushkina, E. A.; Zakharkin, L. I.
Russian Chemical Bulletin, 1994 , vol. 43, # 2 p. 249 - 251
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1994 , # 2 p. 270 - 272
反应条件
isopropylmagnesium chloride; sodium hydride; NiCl2(dppb) in tetrahydrofuran
36 h; Heatingother catalysts; Product distribution;
参考文献
Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1986 , vol. 317, p. 383 - 408
反应条件
samarium diiodide; isopropyl alcohol; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tabuchi, Takanori; Inanaga, Junji; Yamaguchi, Masaru
Tetrahedron Letters, 1986 , vol. 27, # 5 p. 601 - 602
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,4-di(diphenylphosphino)-butane in tetrahydrofuran; water
T=50°C; 24 h; Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Divekar, Sunil; Safi, Mohamed; Soufiaoui, Mohamed; Sinou, Denis
Tetrahedron, 1999 , vol. 55, # 14 p. 4369 - 4376
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium azide in tetrahydrofuran; water
T=50°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Murahashi, Shun-Ichi; Taniguchi, Yuki; Imada, Yasushi; Tanigawa, Yoshio
Journal of Organic Chemistry, 1989 , vol. 54, # 14 p. 3292 - 3303
参考文献
Meinwald,J. et al.
Tetrahedron Letters, 1971 , p. 3485 - 3488