6-氨基-5-溴-1-甲基尿嘧啶合成路线 (共 14 条)
反应条件
bromine; sodium acetate in acetic acid T=20 - 125°C;
参考文献
Balssa, Frederic; Bonnaire, Yves
Journal of Labelled Compounds and Radiopharmaceuticals, 2007 , vol. 50, # 1 p. 33 - 41
参考文献
Journal of the Chemical Society, , p. 917,920
反应条件
1: H2O / 4 h / 70 °C 2: 8 h / Heating View Scheme
参考文献
Zhang, Lei; Zhang, Y. John
Tetrahedron Letters, 2006 , vol. 47, # 5 p. 775 - 778
反应条件
in water T=70°C; 4 h;
参考文献
Mueller, Christa E.; Geis, Uli; Hipp, Jo; Schobert, Ulrike; Frobenius, Wolfram; Pawlowski, Maciej; Suzuki, Fumio; Sandoval-Ramirez, Jesus
Journal of Medicinal Chemistry, 1997 , vol. 40, # 26 p. 4396 - 4405
反应条件
in water T=65°C; 3 h;
参考文献
Rybar, Alfonz; Hesek, Dusan; Szemes, Fridrich; Alfoeldi, Juraj; Tegza, Marian
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, # 9 p. 2257 - 2269
反应条件
T=120°C; 0.166667 h; microwave irradiation;
参考文献
Zhang, Lei; Zhang, Y. John
Tetrahedron Letters, 2006 , vol. 47, # 5 p. 775 - 778
参考文献
Rybar, Alfonz; Hesek, Dusan; Szemes, Fridrich; Alfoeldi, Juraj; Tegza, Marian
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, # 9 p. 2257 - 2269
反应条件
in water T=65°C; 3 h;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 55, # 9 p. 2257 - 2269
参考文献
Rybar, Alfonz; Hesek, Dusan; Szemes, Fridrich; Alfoeldi, Juraj; Tegza, Marian
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, # 9 p. 2257 - 2269
反应条件
T=120°C; 0.166667 h; microwave irradiation;
参考文献
Zhang, Lei; Zhang, Y. John
Tetrahedron Letters, 2006 , vol. 47, # 5 p. 775 - 778