2-苯基亚硫酰基乙酸甲酯合成路线 （共 24 条）
反应条件
Aliquatreg; 336; potassium carbonate; potassium iodide in acetonitrile 1.) room temperature, 2.) 60 deg C, 10 h;
参考文献
Chong-ying, Xu; Guang-jian, Liu; Zhen, Zhang
Synthetic Communications, 1987 , vol. 17, # 15 p. 1839 - 1844
反应条件
Aliquatreg; 336; potassium carbonate; potassium iodide in N,N-dimethyl-formamide 1.) room temperature, 2.) 60 deg C, 9 h;
参考文献
Chong-ying, Xu; Guang-jian, Liu; Zhen, Zhang
Synthetic Communications, 1987 , vol. 17, # 15 p. 1839 - 1844
反应条件
1-iodyl-2-nitro-benzene; bis(acetylacetonate)oxovanadium in benzene T=80°C; 6 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 45, p. 31 - 34
反应条件
Aliquatreg; 336; potassium carbonate; potassium iodide in N,N-dimethyl-formamide 1.) 30 min, room temperature, 2.) 60 deg C, 9 h;
参考文献
Chong-ying, Xu; Guang-jian, Liu; Zhen, Zhang
Synthetic Communications, 1987 , vol. 17, # 15 p. 1839 - 1844
反应条件
sodium hydride 1) DMF, 20 deg C, 0.2 h, 2) toluene, 110 deg C, 15 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Allmendinger, Thomas
Tetrahedron, 1991 , vol. 47, # 27 p. 4905 - 4914
反应条件
1-iodyl-2-nitro-benzene; bis(acetylacetonate)oxovanadium in benzene T=80°C; 6 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 45, p. 31 - 34
反应条件
sodium hydride; zinc(II) chloride 1.) THF, 0 deg C to room temperature, 30 min, 2.) THF, a) room temperature, 15-18 h, b) reflux, 30 min; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 11 p. 2683 - 2686
反应条件
rhenic(VII) acid; benzo[1,3,2]dioxaborole in tetrahydrofuran T=20°C; 0.0833333 h; chemoselective reaction;
参考文献
Cabrita, Ivania; Sousa, Sara C.A.; Fernandes, Ana C.
Tetrahedron Letters, 2010 , vol. 51, # 47 p. 6132 - 6135
反应条件
magnesium methanolate in methanol
Ambient temperature;
参考文献
Cass, Quezia B.; Jaxa-Chamiec, Albert A.; Sammes, Peter G.
Journal of the Chemical Society, Chemical Communications, 1981 , # 24 p. 1248 - 1250
反应条件
piperidine in acetonitrile
3 h; Ambient temperature;
参考文献
Tanikaga, Rikuhei; Nozaki, Yoshihito; Tamura, Tadashi; Kaji, Aritsune
Synthesis, 1983 , # 2 p. 134 - 135
