1-(2-O,3-O,5-O-三乙酰基-beta-D-阿拉伯呋喃糖基)-2,4(1H,3H)-嘧啶二酮合成路线 （共 11 条）
反应条件
Lawesson's reagent in 1,4-dioxane 3 h; Heating;
参考文献
Johar, Monika; Manning, Tracey; Tse, Christopher; Desroches, Nancy; Agrawal; Kunimoto, Dennis Y.; Kumar, Rakesh
Journal of Medicinal Chemistry, 2007 , vol. 50, # 15 p. 3696 - 3705
反应条件
keratinase from Paecilomyces marquandii pH=8; 216 h; aq. phosphate bufferEnzymatic reaction;
参考文献
Sabaini, Maria B.; Zinni, Maria A.; Mohorcic, Martina; Friedrich, Jozefa; Iribarren, Adolfo M.; Iglesias, Luis E.
Journal of Molecular Catalysis B: Enzymatic, 2010 , vol. 62, # 3-4 p. 225 - 229
反应条件
1: 70 percent / I2; ceric(IV) ammonium nitrate / acetonitrile / 1 h / 80 °C 2: 80 percent / NaOMe / methanol / 0.5 h / 20 °C View Scheme
参考文献
Lin, Kun-I.; Chiang, Li-Wu; Wu, Chien-Hung; Chen, Shao-Wei; Yu, Chung-Shan
Journal of the Chinese Chemical Society, 2007 , vol. 54, # 2 p. 563 - 568
反应条件
1: Lawesson's reagent / dioxane / 3 h / Heating 2: 400 mg / NH3 / methanol / 3 h / 20 °C View Scheme
参考文献
Johar, Monika; Manning, Tracey; Tse, Christopher; Desroches, Nancy; Agrawal; Kunimoto, Dennis Y.; Kumar, Rakesh
Journal of Medicinal Chemistry, 2007 , vol. 50, # 15 p. 3696 - 3705
反应条件
1: 89 percent / acetonitrile / 1.5 h / Ambient temperature 2: 93 percent / ethanol / 2 h / Ambient temperature View Scheme
参考文献
Divakar, K.J.; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1171 - 1176
反应条件
1: 89 percent / acetonitrile / 1.5 h / Ambient temperature 2: aq.ammonia / dioxane / 6 h / Ambient temperature 3: methanolic ammonia / 16 h / Ambient temperature View Scheme
参考文献
Divakar, K.J.; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1171 - 1176
反应条件
1: 89 percent / acetonitrile / 1.5 h / Ambient temperature
2: aq.ammonia / dioxane / 6 h / Ambient temperature
View Scheme
参考文献
Divakar, K.J.; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1171 - 1176
反应条件
1: 89 percent / acetonitrile / 1.5 h / Ambient temperature
2: dioxane; ethanol / 1.5 h / Ambient temperature
3: methanolic ammonia / 16 h / Ambient temperature
View Scheme
参考文献
Divakar, K.J.; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1171 - 1176
反应条件
1: 89 percent / acetonitrile / 1.5 h / Ambient temperature
2: dioxane / 2 h / Ambient temperature
3: methanolic ammonia / 16 h / Ambient temperature
View Scheme
参考文献
Divakar, K.J.; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1171 - 1176
反应条件
1: 89 percent / acetonitrile / 1.5 h / Ambient temperature
2: pyridine / 4.5 h / Heating
3: methanolic ammionia / 16 h / Ambient temperature
View Scheme
参考文献
Divakar, K.J.; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1171 - 1176
