in tetrahydrofuran addn. of AlCl3 to Bu4NBH4 (molar ratio B:Al=1:2 or 1:3); or addn. of Bu4NBH4 to AlCl3 (molar ratio B:Al=5:1 to 2:1); not isolated, detd. by (11)B-NMR spectrocopy;
参考文献
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), , vol. 39, p. 1119 - 1128
Zhurnal Neorganicheskoi Khimii, , vol. 39, p. 1173 - 1183
1: in tetrahydrofuran Heating / reflux; 2: With sodium hydrogencarbonate in tetrahydrofuran; water
参考文献
Baxter, Ellen W.; Reitz, Allen B.; Parker, Michael H.; Huang, Yifang; Ho, Chih Yung; Strobel, Eric D.; Reynolds, Charles H.
Patent: US2007/232630 A1, 2007 ;
Location in patent: Page/Page column 22 ;
US 20070232630 A1