2-(2-氨基苯基硫代)苯甲腈合成路线 （共 4 条）
反应条件
1: 2-amino-benzenethiol With potassium carbonate in N,N-dimethyl-formamide T=80 - 90°C; 1 h; 2: ortho-chloro-benzonitrile in N,N-dimethyl-formamide T=90°C; 4 h;
参考文献
FERMION OY
Patent: WO2009/95529 A1, 2009 ;
Location in patent: Page/Page column 9 ;
反应条件
hydrogenchloride in methanol; N,N-dimethyl-formamide
参考文献
Nippon Shinyaku Company, Limited
Patent: US5399703 A1, 1995 ;
US 5399703 A
反应条件
sodium hydride 1.) DMF, 0.5 h, 2.) DMF, 120 deg C, 4 h; Yield given. Multistep reaction;
参考文献
Glaxo Wellcome Inc.
Patent: US5607929 A1, 1997 ;
反应条件
acetic acid in anhydrous xylene; water
参考文献
Glaxo Wellcome Inc.
Patent: US5607929 A1, 1997 ;
