3,5-二叔丁基-4-羟基苯乙酮合成路线 （共 20 条）
反应条件
C5CoN5O2(3-)*3C36H30NP2(1+) in dichloromethane T=0°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 21, p. 4849 - 4852
反应条件
potassium tert-butylate; oxygen in N,N-dimethyl-formamide 1.5 h; Ambient temperaturevar. reagents, solvents, temp., other t-butylphenols; MechanismProduct distribution;
参考文献
Journal of Organic Chemistry, , vol. 51, # 12 p. 2257 - 2266
参考文献
Journal of the Chemical Society, , p. 2753
反应条件
1: diethyl ether / 2.5 h / Heating 2: CH3COOH / 0.17 h / Heating View Scheme
参考文献
Nishinaga, Akira; Iwasaki, Hitoshi; Shimizu, Tadashi; Toyoda, Yasushi; Matsuura, Teru
Journal of Organic Chemistry, 1986 , vol. 51, # 12 p. 2257 - 2266
反应条件
(i) Mg, Et2O, (ii) /BRN= 790500/, nBu2O; Multistep reaction;
参考文献
Kahovec,J. et al.
Collection of Czechoslovak Chemical Communications, 1971 , vol. 36, p. 1986 - 1994
反应条件
1: 100 percent / TiCl4 / benzene / 48 h / Ambient temperature 2: O2, Co(Salpr) / CH2Cl2 / 4.5 h / Ambient temperature View Scheme
参考文献
Nishinaga, Akira; Shimizu, Tadashi; Toyoda, Yasushi; Matsuura, Teruo; Hirotsu, Ken
Journal of Organic Chemistry, 1982 , vol. 47, # 12 p. 2278 - 2285
反应条件
2,6-dimethylpyridine; sodium perchlorate anodic oxidation;
参考文献
Chemische Berichte, , vol. 115, # 1 p. 288 - 308
反应条件
bromine in ethanol 2.5 h;
参考文献
Zhang, Kai; Corrie, John E. T.; Munasinghe, V. Ranjit N.; Wan, Peter
Journal of the American Chemical Society, 1999 , vol. 121, # 24 p. 5625 - 5632
反应条件
1: 56 percent / iodine / 2 h / Heating 2: 80 percent / sodium hydroxide / ethanol; H2O / 1 h / Heating View Scheme
参考文献
Abaev, V. T.; Bumber, A. A.; Okhlobystin, O. Yu.
J. Gen. Chem. USSR (Engl. Transl.), 1987 , vol. 57, # 4 p. 827 - 831,731 - 734
反应条件
sulfuryl dichloride in dichloromethane
参考文献
Hoechst Aktiengesellschaft
Patent: US4940790 A1, 1990 ;
