反应条件
1: methyl-1,2,5-tribromobenzene With isopropylmagnesium chloride in tetrahydrofuran
T=-40°C; Grignard reaction; 2 h;
2: carbon dioxide in tetrahydrofuran
T=-40°C; 1 h; Further stages. Title compound not separated from byproducts.;
参考文献
Menzel, Karsten; Mills, Paul M.; Frantz, Doug E.; Nelson, Todd D.; Kress, Michael H.
Tetrahedron Letters, 2008 , vol. 49, # 3 p. 415 - 418
