1-叠氮-1-脱氧-β-D-吡喃半乳糖苷四乙酸酯合成路线 （共 22 条）
反应条件
sodium azide; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate in dichloromethane
参考文献
Wang, Shuai; Cuesta-Seijo, Jose A.; Lafont, Dominique; Palcic, Monica M.; Vidal, Sebastien
Chemistry - A European Journal, 2013 , vol. 19, # 45 p. 15346 - 15357
反应条件
trimethylsilylazide; tin(IV) chloride in hexane; dichloromethane; ethyl acetate
参考文献
Alchemia Pty LTD
Patent: US6573337 B1, 2003 ;
反应条件
trimethylsilylazide; silver perchlorate; tin(IV) chloride in dichloromethane; toluene 3 h; Ambient temperature;
参考文献
Murphy, Paul V.; Bradley, Helena; Tosin, Manuela; Pitt, Nigel; Fitzpatrick, Geraldine M.; Glass, W. Kenneth
Journal of Organic Chemistry, 2003 , vol. 68, # 14 p. 5692 - 5704
反应条件
1: With hydrogen bromide in dichloromethane; acetic acid T=0°C; Inert atmosphere; 2: With sodium azide in N,N-dimethyl-formamide T=20°C; 3 h; Inert atmosphere;
参考文献
European Journal of Medicinal Chemistry, , vol. 63, p. 782 - 792
反应条件
1: With hydrogen bromide in acetic acid T=0 - 20°C; 0.25 h; 2: With hydrogen bromide in acetic acid T=0 - 20°C; 2 h; 3: With sodium azide; tetra(n-butyl)ammonium hydrogensulfate; sodium carbonate in dichloromethane T=20°C; 1.5 h;
参考文献
Kumar, Rishi; Tiwari, Pallavi; Maulik, Prakas R.; Misra, Anup K.
European Journal of Organic Chemistry, 2006 , # 1 p. 74 - 79
反应条件
trimethylsilylazide; tetrabutyl ammonium fluoride
参考文献
Journal of Organic Chemistry, , vol. 72, # 12 p. 4547 - 4550
反应条件
sodium azide in N,N-dimethyl-formamide 1) 50 deg C, 2 h, 2) 70 deg C, 1 h;
参考文献
Sabesan; Neira
Carbohydrate Research, 1992 , vol. 223, p. 169 - 185
反应条件
in N-methyl-acetamide
反应条件
sodium azide; acetonitrile
参考文献
Justus Liebigs Annalen der Chemie, , vol. 498, p. 50,55
反应条件
tetra-N-butylammonium azide in tetrahydrofuran 60 h; Reflux;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 20, # 14 p. 4263 - 4265
