in sulfuric acid oxidn. react. of suspn. RuO2*nH2O in aq. H2SO4 with Cr2O7(2-) in aq. H2SO4 under N2;
参考文献
Mills, Andrew; Giddings, Susan; Patel, Ila
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1987 , vol. 83, # 8 p. 2317 - 2330
Woehler, L.; Metz, L.
Z. Anorg. Chem., 1925 , vol. 149, p. 298 - 298
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Woehler, L.; Metz, L.
Z. Anorg. Chem., 1925 , vol. 149, p. 299 - 299
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Gmelin Handbook: Te: MVol., 64, page 232 - 234
in water
the soln. of the ligand is added to the soln. of Cr2O7(2-) at pH4.8; violet complex is extd. with CHCl3 and charged to a column of silica gel and eluated with CHCl3, the violet complex is freed from solvent by evapn., the solid is recrystd. from CHCl3, thin layer chromy. on silica gel, elem. anal.;
参考文献
Soundararajan, G.; Subbaiyan, M.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1983 , vol. 22, # 12 p. 1058 - 1061
Stiasny, E.; Das, B. M.
Journal of the Society of Chemical Industry, London, 1912 , vol. 31, p. 753 - 759
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Gmelin Handbook: S: MVol.B2, 11, page 992 - 1010
