3-乙酰基噻吩-2-磺酰胺合成路线 (共 4 条)
反应条件
hydrogenchloride in tetrahydrofuran 1 h; Reflux;
参考文献
AUSPEX PHARMACEUTICALS, INC.
Patent: US2010/317655 A1, 2010 ;
Location in patent: Page/Page column 15 ;
反应条件
in tetrahydrofuran; hydrogenchloride
参考文献
Alcon Laboratories, Inc.
Patent: US5538966 A1, 1996 ;
反应条件
1: With toluene-4-sulfonic acid in acetonitrile T=20°C; 0.5 h; 2: With N-bromosuccinmide in acetonitrile 2 h; Heating / reflux;
参考文献
Sathe, Dhananjay Govind; Tarur, Radhakrishnan Venkatasubramanian; Bhise, Nandu Baban; Shinde, Ajit Bhaskar; Pardeshi, Santosh
Patent: US2010/9977 A1, 2010 ;
Location in patent: Page/Page column 11 ;
反应条件
sodium borohydride; pyridinium hydrobromide perbromide in tetrahydrofuran; ethanol; water
参考文献
Alcon Laboratories, Inc.
Patent: US5153192 A1, 1992 ;