三甲基(环己基氧基)硅烷合成路线 (共 49 条)
反应条件
tin(II) trifluoromethanesulfonate; dimethyl tert-butyl silane in acetonitrile
T=-20°C;
参考文献
Suzuki, Takeshi; Oriyama, Takeshi
Synthetic Communications, 1999 , vol. 29, # 8 p. 1263 - 1269
反应条件
trimethylsilyl trifluoromethanesulfonate in chloroform
T=20°C; 4 h;
参考文献
Kobashi, Yohei; Minowa, Tomofumi; Mukaiyama, Teruaki
Chemistry Letters, 2004 , vol. 33, # 10 art. no. CL-040929, p. 1362 - 1363
反应条件
triethylsilane; trimethylsilyl trifluoromethanesulfonate in dichloromethane
T=-78 - -30°C;
参考文献
Hatakeyama, Susumi; Mori, Hisato; Kitano, Kaori; Yamada, Hidetoshi; Nishizawa, Mugio
Tetrahedron Letters, 1994 , vol. 35, # 25 p. 4367 - 4370
反应条件
di-tert-butyl peroxide
参考文献
Baratchart,M. et al.
Bulletin de la Societe Chimique de France, 1976 , p. 953 - 956
反应条件
triethylsilane; trimethylsilyl trifluoromethanesulfonate in dichloromethane
0 deg C -> r.t.;
参考文献
Hatakeyama, Susumi; Mori, Hisato; Kitano, Kaori; Yamada, Hidetoshi; Nishizawa, Mugio
Tetrahedron Letters, 1994 , vol. 35, # 25 p. 4367 - 4370
反应条件
trimethylsilyl trifluoromethanesulfonate in chloroform
T=-60 - 0°C; 3 h;
参考文献
Kobashi, Yohei; Minowa, Tomofumi; Mukaiyama, Teruaki
Chemistry Letters, 2004 , vol. 33, # 10 art. no. CL-040929, p. 1362 - 1363
反应条件
(Ppyz)Zr(BH4)2Cl2 in diethyl ether
T=20°C; 9 h;
参考文献
Tajbakhsh; Lakouraj; Shirini; Habibzadeh; Nikdoost
Tetrahedron Letters, 2004 , vol. 45, # 16 p. 3295 - 3299
反应条件
manganese(IV) oxide; aluminium trichloride in acetonitrile
Oxidation; 1 h; Heating;
参考文献
Firouzabadi, Habib; Etemadi, Shahrad; Karimi, Babak; Jarrahpour, Ali Asghar
Synthetic Communications, 1999 , vol. 29, # 24 p. 4333 - 4339
反应条件
T=37°C; 45percent acetone-containing aqueous buffer; Rate constant;
参考文献
Shirai, Naohiro; Moriya, Kiyoshi; Kawazoe, Yutaka
Tetrahedron, 1986 , vol. 42, # 8 p. 2211 - 2214