in solid matrix Kinetics; Irradiation (UV/VIS); 16-24 K, solid Ar; IR spectroscopy;
参考文献
Misochko, Eugenii Ya.; Akimov, Alexander V.; Goldschleger, Ilya U.; Boldyrev, Alexander I.; Wight, Charles A.
Journal of the American Chemical Society, 1999 , vol. 121, # 2 p. 405 - 410
Bartlett, N.; Beaton, S. P.; Jha, N. K.
Chemical Communications (London), 1966 , p. 168 - 169
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Gmelin Handbook: Os: SVol.1, 3.3.3.2, page 121 - 121
in neat (no solvent) cylinder fiited with dry powdered element, NF3O condensed into cylinder at -196°C, mixt. heated at 200°C for 24h; not isolated, monitored by NMR, IR;
参考文献
Gupta, O. D.; Kirchmeier, Robert L.; Shreeve, Jean'ne M.
Inorganic Chemistry, 1990 , vol. 29, p. 573 - 574
in neat (no solvent) byproducts: CF3COCF2NF2; NF3O and CF2C(CF3)BF2 were combined at -196°C in a Pyrex reactor, warmed to room temp., cooling-warming was repeated several times; sepd. by fractional condensation;
参考文献
Wilson, Richard D.; Maya, Walter; Pilipovich, Donald; Christe, Karl O.
Inorganic Chemistry, 1983 , vol. 22, p. 1355 - 1358
in neat (no solvent) cylinder fiited with dry powdered element, NF3O condensed into cylinder at -196°C, mixt. heated at 200°C for 24h; not isolated, monitored by NMR, IR;
参考文献
Gupta, O. D.; Kirchmeier, Robert L.; Shreeve, Jean'ne M.
Inorganic Chemistry, 1990 , vol. 29, p. 573 - 574
in neat (no solvent) cylinder fiited with dry powdered element, NF3O condensed into cylinder at -196°C, mixt. heated at 220°C for 36h; not isolated, monitored by NMR, IR;
参考文献
Gupta, O. D.; Kirchmeier, Robert L.; Shreeve, Jean'ne M.
Inorganic Chemistry, 1990 , vol. 29, p. 573 - 574
