1-甲基-4-(1-甲基乙烯基)环己醇合成路线 (共 16 条)
反应条件
sodium in tetrahydrofuran T=65°C; 14 h;
参考文献
Gurudutt, K. N.; Pasha, M. A.; Ravindranath, B.; Srinivas, P.
Tetrahedron, 1984 , vol. 40, # 9 p. 1629 - 1632
反应条件
n-butyllithium; potassium tert-butylate in hexane T=60°C; 48 h;
参考文献
Deagostino; Tivola; Prandi; Venturello
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 21 p. 2856 - 2860
反应条件
tert.-butylhydroperoxide in decane; toluene T=109.84°C; 24 h; Catalytic behavior; Reagent/catalystSolventTemperature; Overall yield = 96 percent;
参考文献
Fernandes, Cristina I.; Carvalho, Maria Deus; Ferreira, Liliana P.; Nunes, Carla D.; Vaz, Pedro D.
Journal of Organometallic Chemistry, 2014 , vol. 760, p. 2 - 10
参考文献
Stephan; Helle
Chemische Berichte, 1902 , vol. 35, p. 2149
Full Text Show Details
Schimmel and Co.
Bericht vom April 1901, S. 78; C. 1901 I, 1008
反应条件
bei der Einw. von wasserabspaltenden Mitteln; dl-α-terpineol;
参考文献
Ono
Memoirs of the College of Science, Kyoto Imperial University, vol. <A> 9, p. 75
Chem. Zentralbl., 1926 , vol. 97, # I p. 1401
反应条件
lithium in ethylenediamine 1.5 h; other tri- and tetrasubstituted oxiranes, other time; Mechanism;
参考文献
Gurudutt; Rao; Shaw
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 3 p. 345 - 346
反应条件
T=500°C; TemperatureReagent/catalystSolvent;
参考文献
Leiner, Janne; Stolle, Achim; Ondruschka, Bernd; Netscher, Thomas; Bonrath, Werner
Molecules, 2013 , vol. 18, # 7 p. 8358 - 8375
反应条件
tert.-butylhydroperoxide; toluene-4-sulfonic acid in acetonitrile T=79.9°C; Product distribution;
参考文献
Corma, A.; Iglesias, M.; Sanchez, F.
Journal of the Chemical Society, Chemical Communications, 1995 , # 16 p. 1635 - 1636
反应条件
oxalic acid in water T=100°C; 4 h; oth. acid, oth. time; Product distribution;
参考文献
Botkina, S. S.; Gankin, V. Yu.; Rubinshtein, E. I.; Sinitsyn, A. V.; Skop, S. L.; et al.
J. Appl. Chem. USSR (Engl. Transl.), 1980 , vol. 53, # 12 p. 2721 - 2726,2061 - 2065
参考文献
Perkin
Journal of the Chemical Society, 1904 , vol. 85, p. 660