反应条件
1: 94 percent / imidazole / CH2Cl2 2: 97 percent / DIBAL / tetrahydrofuran / 0 °C 3: 92 percent / n-Bu3P / tetrahydrofuran / Ambient temperature 4: 1.) m-chloroperoxybenzoic acid; 2.) TFAA, 2,6-lutidine / 1.) CH2Cl2, 0 deg C; 2.) CH2Cl2 5: 59 percent / NaClO2, Na2PO4, 2-methyl-2-butene / H2O; 2-methyl-propan-2-ol 6: 53 percent / TFA / H2O View Scheme
参考文献
Tetrahedron Letters, , vol. 39, # 33 p. 6027 - 6028
