sulfuric acid; iodine cloride T=80°C; Iodination; 2 h;

diethyl ether; ammonia; sodium amide

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ammonium hydroxide; copper(I) bromide T=180°C;

T=180°C;

1: 93 percent / tri-o-tolylphosphine, palladium(II) acetate, Et3N / dimethylformamide / 0.5 h / 95 °C 2: ethanol. NaOH / 2 h / Heating 3: H2 / 10percent Pd-C / H2O / 4 h / 2585.7 - 2844.3 Torr / Ambient temperature 4: 9 percent / 3A molecular sieves / 50 h / Heating View Scheme

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