反应条件
in hydrogen fluoride HF (liquid); OsF6 dissolved in anhydrous HF, cooled the Kel-F-tube to -196°C, PF3 added, tube placed in an acetone-solid CO2 cold bath, maintained for a long period at -78°C, allowed to warm to room temp. for 12 h; votlatile species removed, fractionation; elem. anal.; IR;
参考文献
Burns, R. C.; O'Donnell, T. A.
Journal of Inorganic and Nuclear Chemistry, 1980 , vol. 42, p. 1285 - 1292
