Timakov, A. A.; Prusakov, V. N.; Drobyshevskii, Yu. V.
Kinetics and Catalysis, 1982 , vol. 23, p. 889 - 892
Kinetika i Kataliz, 1982 , vol. 23, p. 1048 - 1051
Knorre, G. v.
Angewandte Chemie, 1902 , vol. 15, p. 395 - 395
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Orlow, N. A.
Chemiker-Zeitung, 1906 , vol. 30, p. 714 - 714
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Gmelin Handbook: Os: MVol., 17, page 31 - 33
CS2 in neat (no solvent) byproducts: CF4; large exess of CS2 condensed onto hexafluoride at -196°C, allowed to warm slowly to room temp.; volatile species removed, fractionated; IR;
参考文献
Burns, R. C.; O'Donnell, T. A.
Journal of Inorganic and Nuclear Chemistry, 1980 , vol. 42, p. 1285 - 1292
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反应条件
in neat (no solvent) byproducts: BF3; 5percent excess of OsF6 added at liquid-nitrogen temp. to B2S3, heated at 210°C for 4-6 h; volatiles determined by IR, solids did by X-ray powder diffraction;
参考文献
Holloway, John. H; Rook, John
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1987 , p. 2285 - 2288
in neat (no solvent) 5percent excess of OsF6 added at liquid-nitrogen temp. to ZnS, heated at 300°C for 7-11 h; volatiles determined by IR, solids did by X-ray powder diffraction;
参考文献
Holloway, John. H; Rook, John
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1987 , p. 2285 - 2288
→
反应条件
in neat (no solvent) byproducts: BF3; 5percent excess of OsF6 added at liquid-nitrogen temp. to B2S3, heated at 210°C for 4-6 h; volatiles determined by IR, solids did by X-ray powder diffraction;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 2285 - 2288
