1,5,6,7-四氢-4H-吲哚-4-酮合成路线 (共 29 条)
反应条件
ammonium hydroxide in ethanol T=150°C; 12 h;
参考文献
Matsumoto, Masakatsu; Watanabe, Nobuko
Heterocycles, 1984 , vol. 22, # 10 p. 2313 - 2316
反应条件
Me2NH*BH3; potassium carbonate; triphenylphosphine; NiCl2((PPh3)P)2 in acetonitrile T=40°C; 8 h;
参考文献
Lipshutz, Bruce H.; Pfeiffer, Steven S.; Reed, Anthony B.
Organic Letters, 2001 , vol. 3, # 26 p. 4145 - 4148
参考文献
Kuraray Co., Ltd.
Patent: US4336202 A1, 1982 ;
反应条件
trifluoroacetic acid in dichloromethane T=0 - 20°C; 12 h;
参考文献
Bellur, Esen; Yawer, Mirza A.; Hussain, Ibrar; Riahi, Abdolmajid; Fatunsin, Olumide; Fischer, Christine; Langer, Peter
Synthesis, 2009 , # 2 p. 227 - 242
反应条件
tetrakis(triphenylphosphine) palladium(0); 2-Bromo-1,3,5-trimethyl-benzene; potassium carbonate in N,N-dimethyl-formamide T=150°C; 4 h;
参考文献
Aoyagi, Yutaka; Mizusaki, Toshihiko; Shishikura, Masahiro; Komine, Takashi; Yoshinaga, Tokuji; Inaba, Haruko; Ohta, Akihiro; Takeya, Koichi
Tetrahedron, 2006 , vol. 62, # 36 p. 8533 - 8538
反应条件
1: 60 percent / molecular sieves 4 Angstroem / tetrahydrofuran / 6 h / Heating 2: 63 percent / Pd(PPh3)4; K2CO3; mesityl bromide / dimethylformamide / 4 h / 150 °C View Scheme
参考文献
Tetrahedron, , vol. 62, # 36 p. 8533 - 8538
反应条件
sodium periodate in water
参考文献
Dianez, Maria J.; Galan, Jose; Gomez-Sanchez, Antonio; Lopez-Castro, Amparo; Rico, Manuel
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 581 - 588
反应条件
H5[PMo11VO40] T=20°C; 6 h; Neat (no solvent);
参考文献
Hekmatshoar, Rahim; Sadjadi, Sodeh; Sadjadi, Samaheh; Heravi, Majid M.; Beheshtiha, Yahya S.; Bamoharram, Fatemeh F.
Synthetic Communications, 2010 , vol. 40, # 11 p. 1708 - 1716
反应条件
(NH4)2CO3 in methanol T=150°C; 40 h; Yield given;
参考文献
Chemistry Letters, , p. 1603 - 1604
反应条件
(NH4)2CO3 in methanol T=150°C; 40 h; Yield given;
参考文献
Chemistry Letters, , p. 1603 - 1604