1-甲氧基-2-(甲基磺酰基)苯合成路线 （共 20 条）
反应条件
hydrogen bromide T=150°C;
参考文献
Forest Laboratories Holdings Limited
Patent: US2009/239810 A1, 2009 ;
Location in patent: Page/Page column 68 ;
US 20090239810 A1
反应条件
3-chloro-benzenecarboperoxoic acid
参考文献
Marcos, Carlos F.; Perrio, Stephane; Slawin, Alexandra M. Z.; Thomas, Susan E.; Williams, David J.
Journal of the Chemical Society, Chemical Communications, 1994 , # 6 p. 753 - 754
反应条件
oxygen; copper diacetate; silver carbonate in N,N-dimethyl-formamide
T=145°C; 18 h;
参考文献
Bhadra, Sukalyan; Dzik, Wojciech I.; Goossen, Lukas J.
Synthesis (Germany), 2013 , vol. 45, # 17 art. no. SS-2013-Z0414-PSP, p. 2387 - 2390
反应条件
phosphate buffer; dihydrogen peroxide; chiral Al(salalen) in methanol
T=20°C; 24 h;
参考文献
Yamaguchi, Tetsufumi; Matsumoto, Kazuhiro; Saito, Bunnai; Katsuki, Tsutomu
Angewandte Chemie - International Edition, 2007 , vol. 46, # 25 p. 4729 - 4731
反应条件
dihydrogen peroxide; (Ra,S,S,Ra)-Al(salalen) in phosphate buffer
T=0°C; pH=7.4; 24 h;
参考文献
Matsumoto, Kazuhiro; Yamaguchi, Tetsufumi; Katsuki, Tsutomu
Chemical Communications, 2008 , # 14 p. 1704 - 1706
反应条件
alpha,alpha-dimethylbenzyl hydroperoxide; 4 A molecular sieve; titanium(IV) isopropylate; (3S,4S)-2,2,5,5-tetramethyl-3,4-hexanediol in toluene
T=-20°C; Oxidation; 60 h; Title compound not separated from byproducts;
参考文献
Yamanoi, Yoshinori; Imamoto, Tsuneo
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8560 - 8564
反应条件
dihydrogen peroxide; titanium binaphthyl-bridged Schiff base
T=20°C; 0.25 h;
参考文献
De Rosa, Margherita; Lamberti, Marina; Pellecchia, Claudio; Scettri, Arrigo; Villano, Rosaria; Soriente, Annunziata
Tetrahedron Letters, 2006 , vol. 47, # 40 p. 7233 - 7235
反应条件
1.1: MeLi / tetrahydrofuran / -78 °C
1.2: N-phenylsulfonyl-phenyloxaziridine / -78 °C
1.3: H2O / ethyl acetate
2.1: nBu4NBr / H2O; toluene; acetone / Heating
View Scheme
参考文献
Sandrinelli, Franck; Perrio, Stephane; Beslin, Pierre
Phosphorus, Sulfur and Silicon and Related Elements, 1999 , vol. 153-154, p. 381 - 382
参考文献
Troeger; Budde
Journal fuer Praktische Chemie (Leipzig), 1902 , vol. <2> 66, p. 139
反应条件
tetrabutylammomium bromide in water; acetone; toluene
Methylation; Heating;
参考文献
Sandrinelli, Franck; Perrio, Stephane; Beslin, Pierre
Phosphorus, Sulfur and Silicon and Related Elements, 1999 , vol. 153-154, p. 381 - 382
