(4-甲基苯基)-1-哌啶基-甲酮合成路线 (共 45 条)
反应条件
Zr(NMe2)4 in toluene T=50°C; 5 h; Inert atmosphere;
参考文献
Stephenson, Nickeisha A.; Zhu, Jiang; Gellman, Samuel H.; Stahl, Shannon S.
Journal of the American Chemical Society, 2009 , vol. 131, # 29 p. 10003 - 10008
反应条件
Al2(NMe2)6 in toluene T=90°C; 16 h; Equilibrium constant;
参考文献
Hoerter, Justin M.; Otte, Karin M.; Gellman, Samuel H.; Cui, Qiang; Stahl, Shannon S.
Journal of the American Chemical Society, 2008 , vol. 130, # 2 p. 647 - 654
反应条件
Al2(NMe2)6 in toluene T=90°C; 16 h; Equilibrium constant;
参考文献
Hoerter, Justin M.; Otte, Karin M.; Gellman, Samuel H.; Cui, Qiang; Stahl, Shannon S.
Journal of the American Chemical Society, 2008 , vol. 130, # 2 p. 647 - 654
反应条件
1: piperidine With C24H48KO6(1+)*C108H152KLa2O12(1-)
0.5 h; Inert atmosphere;
2: 4-methyl-benzaldehyde T=25°C; 22 h; Inert atmosphere;
参考文献
Zhu, Mingwen; Fujita, Ken-Ichi; Yamaguchi, Ryohei
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 9102 - 9109,8
反应条件
potassium carbonate in toluene
T=105°C; P=3000.3 Torr; 12 h;
参考文献
Dang, Tuan T.; Zhu, Yinghuai; Ngiam, Joyce S. Y.; Ghosh, Subhash C.; Chen, Anqi; Seayad, Abdul M.
ACS Catalysis, 2013 , vol. 3, # 6 p. 1406 - 1410
反应条件
potassium carbonate; bis[2-(diphenylphosphino)phenyl] ether in toluene
T=105°C; P=3000.3 Torr; 12 h;
参考文献
Dang, Tuan T.; Zhu, Yinghuai; Ngiam, Joyce S. Y.; Ghosh, Subhash C.; Chen, Anqi; Seayad, Abdul M.
ACS Catalysis, 2013 , vol. 3, # 6 p. 1406 - 1410
反应条件
trifluorormethanesulfonic acid
T=50°C; 12 h; Inert atmosphere;
参考文献
Raja, Erum K.; Nilsson Lill, Sten O.; Klumpp, Douglas A.
Chemical Communications, 2012 , vol. 48, # 65 p. 8141 - 8143
反应条件
triethylamine in dichloromethane
T=20°C;
参考文献
Salvio, Riccardo; Moisan, Lionel; Ajami, Dariush; Rebek Jr., Julius
European Journal of Organic Chemistry, 2007 , # 16 p. 2722 - 2728
反应条件
tris(2,4-di-tert-butyl-phenyl) phosphite; potassium methanolate; [Ni(O2CCH3)2]*4H2O in diethylene glycol dimethyl ether
T=110°C; 10 h;
参考文献
Jo, Youngshin; Ju, Jinhun; Choe, Jaehoon; Kwang, Ho Song; Lee, Sunwoo
Journal of Organic Chemistry, 2009 , vol. 74, # 16 p. 6358 - 6361
反应条件
ammonium cerium(IV) nitrate; acetic acid in water
T=20°C; 0.333333 h;
参考文献
Movassagh, Barahman; Meibodi, Forhatosadat; Sobhani, Shahin
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 6 p. 1296 - 1298