(±)-2-甲基-1-丁醇合成路线 （共 128 条）
反应条件
Lipase PS "Amano" in pentane T=20°C; Title compound not separated from byproducts.;
参考文献
Verheggen; Ryne; Olsson; Arnaud; Lognay; Hoegberg; Persson; Haubruge; Loefstedt
Journal of Chemical Ecology, 2007 , vol. 33, # 3 p. 525 - 539
反应条件
ueber den Tartranilsaeureester; teilweise racemisierte Praeparat entsteht;
参考文献
Sagiroglu, Ayten; Telefoncu, Azmi
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 1 p. 85 - 87
反应条件
1: With (R,R,R,R)-(-)-trans,trans-2,3,10,11-tetrakis(hydroxydiphe.. T=20°C; inclusion complexation; resolution of racemate; 24 h; 2: T=180°C; decomposition of complex; P=30 Torr;
参考文献
Tanaka, Koichi; Honke, Shinji; Urbanczyk-Lipkowska, Zofia; Toda, Fumio
European Journal of Organic Chemistry, 2000 , # 18 p. 3171 - 3176
反应条件
Lipase PS "Amano" in pentane T=20°C; Title compound not separated from byproducts.;
参考文献
Verheggen; Ryne; Olsson; Arnaud; Lognay; Hoegberg; Persson; Haubruge; Loefstedt
Journal of Chemical Ecology, 2007 , vol. 33, # 3 p. 525 - 539
反应条件
acetobromo-α-D-glucose Umkrystallisieren aus Aethanol und folgende Spaltung mit methylalkoholischem NH3;
参考文献
Barrow; Atkinson
Journal of the Chemical Society, 1939 , p. 638
反应条件
in water T=35 - 37°C; 140 h; Candida cylindracea lipase immobilized on Amberlite IRA-938, pH 7.3; Yield given. Yields of byproduct given;
参考文献
Sagiroglu, Ayten; Telefoncu, Azmi
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 1 p. 85 - 87
反应条件
hydrogenchloride T=90°C;
参考文献
Olah,G.A. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 22 p. 3872 - 3881
反应条件
1: 82.9 percent / phosphorus tribromide / hot-water bath, 3-5 h 2: 25 percent / potassium hydroxide / ethanol / 10 h / Heating 3: 79 percent / boric acid, conc. sulphuric acid / toluene / 24 h / Heating View Scheme
参考文献
Dong, C. C.; Sun, Z. M.; Li, G. Z.
Molecular Crystals and Liquid Crystals (1969-1991), 1990 , vol. 185, p. 35 - 45
参考文献
Hinton; Nieuwland
Journal of the American Chemical Society, 1930 , vol. 52, p. 2892,2893
反应条件
rhenic(VII) acid in water T=170°C; 4 h; Inert atmosphere;
参考文献
Shiramizu, Mika; Toste, F. Dean
Angewandte Chemie - International Edition, 2013 , vol. 52, # 49 p. 12905 - 12909
Angew. Chem., 2013 , vol. 125, # 49 p. 13143 - 13147,5
