in water byproducts: NaCl; ZnCl2, the thiocarbamate in water, immediately pptn.; filtered hot to remove NaCl and any excess of unreacted thiocarbamate, dried (vac. at 80°C), recrystn. (boiling benzene);
in acetonitrile Electrolysis; 4 h, initial voltage 10 V, Zn anode; product was collected, washed with acetonitrile and then petroleum ether and dried in vacuo; elem. anal.;
参考文献
Geloso, Corrado; Kumar, Rajesh; Lopez-Grado, Jaime Romero; Tuck, Dennis G.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 928 - 932
McCleverty, Jon A.; Spencer, Neil; Bailey, Neil A.; Shackleton, Stephen L.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 1939 - 1944
McCleverty, Jon A.; Spencer, Neil; Bailey, Neil A.; Shackleton, Stephen L.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 1939 - 1944
McCleverty, Jon A.; Spencer, Neil; Bailey, Neil A.; Shackleton, Stephen L.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 1939 - 1944
McCleverty, Jon A.; Spencer, Neil; Bailey, Neil A.; Shackleton, Stephen L.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 1939 - 1944
McCleverty, Jon A.; Spencer, Neil; Bailey, Neil A.; Shackleton, Stephen L.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 1939 - 1944
McCleverty, Jon A.; Spencer, Neil; Bailey, Neil A.; Shackleton, Stephen L.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 1939 - 1944
McCleverty, Jon A.; Morrison, Norman J.; Spencer, Neil; Ashworth, Christopher C.; Bailey, Neil A.; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 1945 - 1957
