Alpha-(氯甲基)-2,4-二氯苯甲醇合成路线 （共 4 条）
反应条件
1: With sodium tetrahydroborate in methanol T=0 - 20°C; 1.5 h; Inert atmosphere; 2: With water in methanol
参考文献
Mangas-Sanchez, Juan; Busto, Eduardo; Gotor-Fernandez, Vicente; Malpartida, Francisco; Gotor, Vicente
Journal of Organic Chemistry, 2011 , vol. 76, # 7 p. 2115 - 2122
反应条件
potassium carbonate; sodium iodide in water; butanone
参考文献
Celgene Corporation
Patent: US6207695 B1, 2001 ;
反应条件
in acetonitrile Reflux;
参考文献
Dulcevscaia, Galina M.; Kravtsov, Victor Ch.; Macaev, Fliur Z.; Duca, Gheorghe G.; Stingachi, Eugenia P.; Pogrebnoi, Serghei I.; Boldescu, Veaceslav V.; Clapco, Steliana F.; Tiurina, Janeta P.; Deseatnic-Ciloci, Alexandra A.; Lipkowski, Janusz; Liu, Shi-Xia; Decurtins, Silvio; Baca, Svetlana G.
Polyhedron, 2013 , vol. 52, p. 106 - 114
反应条件
1.1: acetonitrile / |Reflux 2.1: sodium hydride / 1,4-dioxane; mineral oil / 1 h / 20 °C / |Inert atmosphere; |Reflux 2.2: |Inert atmosphere; |Reflux 3.1: nitric acid / acetone / 12 h View Scheme
参考文献
Dulcevscaia, Galina M.; Kravtsov, Victor Ch.; Macaev, Fliur Z.; Duca, Gheorghe G.; Stingachi, Eugenia P.; Pogrebnoi, Serghei I.; Boldescu, Veaceslav V.; Clapco, Steliana F.; Tiurina, Janeta P.; Deseatnic-Ciloci, Alexandra A.; Lipkowski, Janusz; Liu, Shi-Xia; Decurtins, Silvio; Baca, Svetlana G.
Polyhedron, 2013 , vol. 52, p. 106 - 114
