3,4,5-三羟基苯甲醛合成路线 （共 14 条）
反应条件
1: With pyridine; AlCl3, aluminium chloride in 1,2-dichloro-ethane T=0°C; Reflux; 2: With hydrogenchloride in water; 1,2-dichloro-ethane
参考文献
Ravindran, Jayaraj; Subbaraju, Gottumukkala V.; Ramani, Modukuri V.; Sung, Bokyung; Aggarwal, Bharat B.
Biochemical Pharmacology, 2010 , vol. 79, # 11 p. 1658 - 1666
反应条件
aluminium trichloride in dichloromethane T=20°C; 12 h;
参考文献
Zou, Hong Bin; Dong, Sheng Yi; Zhou, Chang Xin; Hu, Li Hong; Wu, Yi Hang; Li, Hai Bo; Gong, Jing Xu; Sun, Lian Li; Wu, Xiu Mei; Bai, Hua; Fan, Bo Tao; Hao, Xiao Jiang; Stoeckigt, Joachim; Zhao, Yu
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 6 p. 2060 - 2071
反应条件
1: 85 percent / pyridinium chlorochromate / CH2Cl2 / 20 °C 2: 30 percent / AlCl3 / CH2Cl2 / 12 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 14, # 6 p. 2060 - 2071
反应条件
1: 72 percent / LiAlH4 / tetrahydrofuran / Heating 2: 85 percent / pyridinium chlorochromate / CH2Cl2 / 20 °C 3: 30 percent / AlCl3 / CH2Cl2 / 12 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 14, # 6 p. 2060 - 2071
反应条件
chloroform; sodium methylate
参考文献
Chemische Berichte, , vol. 85, p. 1181,1188
反应条件
1: xylene; hydrogen; palladium barium sulfate 2: potassium acetate; alcohol View Scheme
参考文献
Chemische Berichte, , vol. 51, p. 598
反应条件
1: phosphorus pentachloride 2: xylene; hydrogen; palladium barium sulfate 3: potassium acetate; alcohol View Scheme
参考文献
Chemische Berichte, , vol. 51, p. 598
反应条件
KBrO3; hydrogenchloride; potassium bromide in water 12 h; Time;
参考文献
Sharma; Robert, Alice R.
Research on Chemical Intermediates, 2013 , vol. 39, # 7 p. 3251 - 3254
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Koller; Hamburg
Monatshefte fuer Chemie, 1935 , vol. 65, p. 367,373
反应条件
in water 0.25 h; Heating;
参考文献
Hussoin; FitzGerald; Wick
Journal of Pharmaceutical Sciences, 1991 , vol. 80, # 5 p. 416 - 418
