4-[2-(叔丁氧羰基)乙基]-4-氨基戊烷二甲酸二叔丁酯合成路线 （共 4 条）
反应条件
hydrogen in ethanol T=25°C; P=2068.65 Torr; 168 h;
参考文献
King's College London; Ballinger, James Russell; Berry, David; Blower, Philip John; Ma, Yongmin; Mullen, Gregory Edgar David
Patent: US2014/56810 A1, 2014 ;
Location in patent: Paragraph 0130 ;
反应条件
1: 81 percent / Triton-B / 1,2-dimethoxy-ethane; methanol / 2 h / 70 - 80 °C 2: 93 percent / H2 / T-1 Ra Ni / ethanol / 1.25 h / 50 - 55 °C / 3102.9 Torr View Scheme
参考文献
Cruz-Morales, Jorge A.; Guadarrama, Patricia
Journal of Molecular Structure, 2005 , vol. 779, # 1-3 p. 1 - 10
反应条件
triethylamine in diethyl ether T=0°C;
参考文献
Newkome, George R.; Weis, Claus D.; Moorefield, Charles N.; Fronczek, Frank R.
Tetrahedron Letters, 1997 , vol. 38, # 40 p. 7053 - 7056
反应条件
in ethyl acetate
T=20°C; 1 h;
参考文献
Yu, Jianjun; Wang, Limin; Liu, Mingtao; Qiu, Jun; Shen, Qiang; Fang, Lei; Tang, Jun
Chinese Journal of Chemistry, 2012 , vol. 30, # 5 p. 1114 - 1118
