1,1'-[(2E)-2-丁烯-1,4-二基]二苯合成路线 (共 22 条)
反应条件
N,N’-di-tert-butylthiadiaziridine-1,1-dioxide; triphenylphosphine; copper(l) chloride T=65°C; 20 h; Inert atmosphere;
参考文献
Ramirez, Thomas A.; Zhao, Baoguo; Shi, Yian
Tetrahedron Letters, 2010 , vol. 51, # 14 p. 1822 - 1825
反应条件
N,N’-di-tert-butylthiadiaziridine-1,1-dioxide; triphenylphosphine; copper(l) chloride T=65°C; 20 h; Inert atmosphere;
参考文献
Ramirez, Thomas A.; Zhao, Baoguo; Shi, Yian
Tetrahedron Letters, 2010 , vol. 51, # 14 p. 1822 - 1825
反应条件
3,3-dimethylbut-1-yne; sodium t-butanolate; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; 1,3-dimesitylimidazol-2-ylidene chloride in hexane
T=80°C; 8 h;
参考文献
Louie, Janis; Grubbs, Robert H.
Angewandte Chemie, International Edition, 2001 , vol. 40, # 1 p. 247 - 249
Angewandte Chemie, 2001 , vol. 113, p. 253 - 255
反应条件
titanium(III) chloride; iodine; lithium in tetrahydrofuran
T=25°C; 4 h;
参考文献
Talukdar, Sanjay; Nayak, Sandip K.; Banerji, Asoke
Journal of Organic Chemistry, 1998 , vol. 63, # 15 p. 4925 - 4929
反应条件
methanol; ytterbium in tetrahydrofuran
18 h; Ambient temperature;
参考文献
Hou, Zhaomin; Taniguchi, Hiroshi; Fujiwara, Yuzo
Chemistry Letters, 1987 , p. 305 - 308
反应条件
1: With lithium vanadium(I) dihydride in tetrahydrofuran
T=25°C; 12 h; Inert atmosphere;
2: With hydrogenchloride in water
参考文献
Eisch, John J.; Fregene, Paul O.
European Journal of Organic Chemistry, 2008 , # 26 p. 4482 - 4492
反应条件
Rh(ethylene)2(hydrotris(pyrazolyl)borate); dibenzylideneacetone; lithium bromide in diethyl ether
T=0°C; 0.25 h;
参考文献
Evans, P. Andrew; Uraguchi, Daisuke
Journal of the American Chemical Society, 2003 , vol. 125, # 24 p. 7158 - 7159
反应条件
RuCl2(tricyclohexylphosphine)2(benzylidene) in water
T=20°C; 12 h; Micellar solution;
参考文献
Lipshutz, Bruce H.; Aguinaldo, Grant T.; Ghorai, Subir; Voigtritter, Karl
Organic Letters, 2008 , vol. 10, # 7 p. 1325 - 1328
反应条件
triethylamine
1) acetonitrile, -40 deg C, 2) heating; Yield given. Multistep reaction;
参考文献
Opitz, Guenter; Ehlis, Thomas; Rieth, Karlheinz
Chemische Berichte, 1990 , vol. 123, # 10 p. 1989 - 1998
反应条件
RuCl2(9-isobutyl-9-phosphabicyclo-[3.3.1]-nonane)2(3-phenylindenylidene) in dichloromethane
T=25°C; Inert atmosphere;
参考文献
Sauvage, Xavier; Zaragoza, Guillermo; Demonceau, Albert; Delaude, Lionel
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 11-12 p. 1934 - 1948