N’-叔丁氧羰基-L-鸟氨酸合成路线 (共 8 条)
反应条件
hydrogen; palladium on activated charcoal in ethanol 48 h;
参考文献
Nakatani, Takafumi; Konishi, Tomoyuki; Miyahara, Kazumoto; Noda, Naoki
Chemical and Pharmaceutical Bulletin, 2004 , vol. 52, # 7 p. 807 - 809
反应条件
1: L-(+)-ornithine hydrochloride With cupric(II) carbonate in water 2 h; Reflux; 2: di-tert-butyl dicarbonate With sodium hydrogencarbonate in water; acetone T=20°C;
参考文献
Bayryamov, Stanislav G.; Vassilev, Nikolay G.; Petkov, Dimiter D.
Protein and Peptide Letters, 2010 , vol. 17, # 7 p. 889 - 898
参考文献
FEBS Journal, , vol. 280, # 8 p. 1807 - 1817
反应条件
(i) 2CuCO3*Cu(OH)2, (ii) /BRN= 1363586/, MgO; Multistep reaction;
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 81 - 85
反应条件
tris(2,2,2-trifluoroethyl) borate in acetonitrile T=100°C; 5 h; Sealed tube;
参考文献
Lanigan, Rachel M.; Starkov, Pavel; Sheppard, Tom D.
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4512 - 4523
参考文献
Harris, Austin P.; Phillips, Robert S.
FEBS Journal, 2013 , vol. 280, # 8 p. 1807 - 1817
反应条件
1: Nδ-Boc-L-ornithine With N,N-dicyclohexylamine in acetone T=20°C; 2: 1-[[(9H-fluoren-9-ylmethoxy)carbonyl]oxy]-2,5-pyrrolidinedione With sodium carbonate in water; acetonitrile T=0 - 20°C; pH=8; 3: With potassium hydrogensulfate in water; acetonitrile pH=2 - 3;
参考文献
Nowshuddin, Shaik; Rao; Reddy, A. Ram
Synthetic Communications, 2009 , vol. 39, # 11 p. 2022 - 2031
反应条件
2: trifluoroacetic acid / dichloromethane / 0.5 h View Scheme
参考文献
Harris, Austin P.; Phillips, Robert S.
FEBS Journal, 2013 , vol. 280, # 8 p. 1807 - 1817