in dichloromethane
treatment N-(pentafluorosulfanyl)-N-nitro octyl carbamate with NH3 in CH2Cl2 at -40°C; chromy. on Silica gel 60 (CH3CN/CH2Cl2 50/50); elem. anal.;
参考文献
Sitzmann, Michael E.; Gilardi, Richard; Butcher, Ray J.; Koppes, William M.; Stern, Alfred G.; Thrasher, Joseph S.; Trivedi, Nirupam J.; Yang, Zhen-Yu
Inorganic Chemistry, 2000 , vol. 39, # 4 p. 843 - 850
