反应条件
1.1: sodium hydroxide / ethanol / 80 °C / Large scale reaction 1.2: Large scale reaction 2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / water; acetonitrile / 1.5 h / 20 °C 3.1: thionyl chloride; triethylamine / acetonitrile / 3 h / 20 - 22 °C 3.2: 16 h / 20 °C 4.1: formic acid; dihydrogen peroxide / 60 °C View Scheme
参考文献
Moseley, Jonathan D.; Brown, David; Firkin, Catherine R.; Jenkin, Shelley L.; Patel, Bharti; Snape, Evan W.
Organic Process Research and Development, 2008 , vol. 12, # 6 p. 1044 - 1059
