(4-甲基苯基)-1,2-乙二醇合成路线 （共 22 条）
反应条件
oxygen; bismuth mandelate in dimethyl sulfoxide
T=80°C; P=760 Torr; 2.3 h; Rate constant;
参考文献
Boisselier, Veronique Le; Dunach, Elisabet; Postel, Michele
Journal of Organometallic Chemistry, 1994 , vol. 482, # 1-2 p. 119 - 124
反应条件
β-cyclodextrin in water
T=60°C; 8 h;
参考文献
Huang, Kun; Wang, Haiyang; Stepanenko, Viatcheslav; De Jesus, Melvin; Torruellas, Carilyn; Correa, Wildeliz; Ortiz-Marciales, Margarita
Journal of Organic Chemistry, 2011 , vol. 76, # 6 p. 1883 - 1886
反应条件
potassium hydroxide in methanol
T=20°C; 24 h;
参考文献
Prathima, P. Sai; Maheswari, C. Uma; Srinivas; Rao, M. Mohan
Tetrahedron Letters, 2010 , vol. 51, # 44 p. 5771 - 5774
反应条件
1: With water in chloroform
T=40°C;
2: With water; sodium hydroxide in chloroform
T=40°C; 18 h;
参考文献
Jones, Kevin M.; Tomkinson, Nicholas C. O.
Journal of Organic Chemistry, 2012 , vol. 77, # 2 p. 921 - 928
反应条件
sodium azide; 2-(n-morpholino)ethanesulfonic acid; sodium perchlorate in 1,4-dioxane
Ambient temperatureother pH; Rate constantProduct distributionMechanism;
参考文献
Blumenstein, Jeffrey J.; Ukachukwu, Victoria C.; Mohan, Ram S.; Whalen, Dale L.
Journal of Organic Chemistry, 1993 , vol. 58, # 4 p. 924 - 932
反应条件
1: 93 percent / [bmim]Br / 0.67 h / 20 °C
2: 100 percent / NaBH4 / methanol / 20 °C
View Scheme
参考文献
Kamal, Ahmed; Chouhan, Gagan
Tetrahedron Letters, 2004 , vol. 45, # 48 p. 8801 - 8805
反应条件
sodium tetrahydroborate in ethanol
参考文献
Liu, Xiang; Wang, Yi; Gao, Hai Yan; Xu, Jian He
Chinese Chemical Letters, 2012 , vol. 23, # 6 p. 635 - 638
反应条件
1: selenium(IV) oxide / 1,4-dioxane; water / 10 h / Reflux
2: sodium tetrahydroborate / ethanol / 1 h
View Scheme
参考文献
Mahajabeen, Pula; Chadha, Anju
Tetrahedron Asymmetry, 2011 , vol. 22, # 24 p. 2156 - 2160
反应条件
1: potassium tert-butylate / tetrahydrofuran / |Inert atmosphere
2: osmium(VIII) oxide; 4-methylmorpholine N-oxide / |Inert atmosphere
View Scheme
参考文献
Coombs, John R.; Haeffner, Fredrik; Kliman, Laura T.; Morken, James P.
Journal of the American Chemical Society, 2013 , vol. 135, # 30 p. 11222 - 11231
反应条件
1: sodium hydroxide / tetrahydrofuran / 2 h
2: β-cyclodextrin / water / 8 h / 60 °C
View Scheme
参考文献
Huang, Kun; Wang, Haiyang; Stepanenko, Viatcheslav; De Jesus, Melvin; Torruellas, Carilyn; Correa, Wildeliz; Ortiz-Marciales, Margarita
Journal of Organic Chemistry, 2011 , vol. 76, # 6 p. 1883 - 1886
