(4-甲基苯基)-1,2-乙二醇合成路线 (共 22 条)
反应条件
tert-butylhypochlorite; Neutral lead acetate; dibenzoyl peroxide in toluene T=20°C; 0.666667 h;
参考文献
Telvekar, Vikas N.; Mali, Jaishree K.; Dighe, Mahesh G.
Synthetic Communications, 2007 , vol. 37, # 5 p. 865 - 868
反应条件
1: NaOH / 24 h / Heating 2: NaN3 / H2O; dimethylformamide / 48 h / 70 °C 3: Red-Al / toluene View Scheme
参考文献
Barlow, Thomas; Dipple, Anthony
Chemical Research in Toxicology, 1998 , vol. 11, # 1 p. 44 - 53
反应条件
hydrogenchloride T=180 - 185°C;
参考文献
Ishimura
Bulletin of the Chemical Society of Japan, 1941 , vol. 16, p. 252,258
Bulletin of the Chemical Society of Japan, 1943 , vol. 18, p. 200
参考文献
Ishimura
Bulletin of the Chemical Society of Japan, 1941 , vol. 16, p. 252,258
Bulletin of the Chemical Society of Japan, 1943 , vol. 18, p. 200
反应条件
tert.-butylhydroperoxide; potassium tert-butylate in water T=80°C; 8 h;
参考文献
Shaikh, Tanveer Mahammadali; Hong, Fung-E
Tetrahedron, 2013 , vol. 69, # 42 p. 8929 - 8935
反应条件
tert-butylhypochlorite; Neutral lead acetate; dibenzoyl peroxide in toluene T=20°C; 0.666667 h;
参考文献
Synthetic Communications, , vol. 37, # 5 p. 865 - 868
反应条件
1: With formic acid; 2,6-dichloropyridine-N-oxide; Ru(IV)(TDCPP)Cl2 in chloroform
T=20°C; Darkness;
2: With potassium carbonate in methanol
参考文献
Hu, Wen-Xiang; Li, Pei-Rong; Jiang, Gaoxi; Che, Chi-Ming; Chen, Jian
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 18 p. 3190 - 3194
反应条件
sodium tetrahydroborate in ethanol
1 h;
参考文献
Mahajabeen, Pula; Chadha, Anju
Tetrahedron Asymmetry, 2011 , vol. 22, # 24 p. 2156 - 2160
反应条件
sodium tetrahydroborate in methanol
T=20°C;
参考文献
Kamal, Ahmed; Chouhan, Gagan
Tetrahedron Letters, 2004 , vol. 45, # 48 p. 8801 - 8805
反应条件
Fe2(S04)3; water in toluene
T=110°C; 2 h; Ionic liquid;
参考文献
Hu, Yu Lin; Jiang, Hui; Zhu, Jie; Lu, Ming
New Journal of Chemistry, 2011 , vol. 35, # 2 p. 292 - 298