4-甲氧基-3-甲基苯胺合成路线 （共 11 条）
反应条件
hydrogen; palladium 10 on activated carbon in methanol T=20°C; P=760.051 Torr; 16 h;
参考文献
AKZO NOBEL N.V.; PHARMACOPEIA DRUG DISCOVERY, INC.
Patent: WO2006/95014 A1, 2006 ;
Location in patent: Page/Page column 33 ;
WO 2006/095014 A1
反应条件
hydrogenchloride in ethanol; chloroform; water
反应条件
1: With pyridine; trifluorormethanesulfonic acid; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=25°C; Electrochemical reaction; 2: With piperidine in acetonitrile T=80°C; 12 h; Electrochemical reaction;
参考文献
Morofuji, Tatsuya; Shimizu, Akihiro; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2013 , vol. 135, # 13 p. 5000 - 5003
反应条件
1: K2CO3 / acetone 2: N2H4*H2O / Raney-Ni / ethanol View Scheme
参考文献
Tetrahedron, , vol. 34, p. 3611 - 3615
参考文献
Journal of the American Chemical Society, , vol. 41, p. 1457
反应条件
1: KOH-solution 2: hydrochloric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 41, p. 1457
反应条件
2: KOH-solution 3: hydrochloric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 41, p. 1457
反应条件
1: With tin(IV) chloride T=20°C; 2: With cesium hydroxide in ethylene glycol T=160°C; 4 h; Title compound not separated from byproducts;
参考文献
Chemistry Letters, , vol. 32, # 6 p. 548 - 549
参考文献
Justus Liebigs Annalen der Chemie, , vol. 390, p. 175
Chemische Berichte, , vol. 40, p. 1903
参考文献
Justus Liebigs Annalen der Chemie, , vol. 424, p. 300
Justus Liebigs Annalen der Chemie, , vol. 441, p. 303
