反应条件
in neat (no solvent) passing dry Cl2 through a glass tube, filled with Ca-silicide and heated by a electric spiral at 150-250 °C for about 12-14 days, further products;; fractional distillation;;
参考文献
Gmelin Handbook: Si: MVol.B, 242, page 657 - 659
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Schumb, W. C.; Gamble, E. L.
Booth, H. S., Inorganic syntheses, Bd. 1, New York-London 1939, S. 42