1: With hydrogenchloride; sodium nitrite in methanol T=-5°C; 0.25 h; 2: With urea; sodium iodide in methanol T=0 - 50°C; Sandmeyer reaction; 5 h;
参考文献
Vyskocil, Stepan; Lockhart, Stephen C.; Mitchell, William L.; Kocovsky, Pavel
Collection of Czechoslovak Chemical Communications, 2003 , vol. 68, # 5 p. 907 - 916
1.1: aq. NaOH / methanol / 20 h / Heating 2.1: aq. HCl; NaNO2 / methanol / 0.25 h / -5 °C 2.2: 10.8 g / aq. NaI; urea / methanol / 5 h / 0 - 50 °C View Scheme
参考文献
Vyskocil, Stepan; Lockhart, Stephen C.; Mitchell, William L.; Kocovsky, Pavel
Collection of Czechoslovak Chemical Communications, 2003 , vol. 68, # 5 p. 907 - 916
Vyskocil, Stepan; Lockhart, Stephen C.; Mitchell, William L.; Kocovsky, Pavel
Collection of Czechoslovak Chemical Communications, 2003 , vol. 68, # 5 p. 907 - 916
