N-叔丁氧羰基-L-谷氨酸5-苄酯合成路线 （共 35 条）
反应条件
in 1,4-dioxane; water T=0°C;
参考文献
Craighead, Mark; Palin, Ronald; Murray, Neil; Lindsay, Derek
Patent: US2013/225594 A1, 2013 ;
Location in patent: Paragraph 0425; 0426 ;
反应条件
phosphate buffer; Candida antarctica Lipase A in methanol; hexane T=37°C; pH=7.4; 4 h;
参考文献
Fotakopoulou, Irene; Barbayianni, Efrosini; Constantinou-Kokotou, Violetta; Bornscheuer, Uwe T.; Kokotos, George
Journal of Organic Chemistry, 2007 , vol. 72, # 3 p. 782 - 786
反应条件
sodium hydrogen sulphate in ethyl acetate Elimination;
参考文献
Onoprienko; Yelin; Miroshnikov
Russian Journal of Bioorganic Chemistry, 2000 , vol. 26, # 6 p. 361 - 368
反应条件
acetic acid; zinc Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, # 8 p. 2433 - 2438
反应条件
1: DL-glutamic acid; toluene-4-sulfonic acid; benzyl alcohol in benzene Heating; 2: With hydrogen iodide; acetic acid T=50°C; 3: di-tert-butyl dicarbonate With sodium carbonate in water; isopropyl alcohol T=0°C; Further stages.;
参考文献
Chemical communications (Cambridge, England), , # 19 p. 1908 - 1909
反应条件
phosphate buffer; Bacillus subtilis esterase BS2 in methanol; hexane T=37°C; pH=7.4; 1 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 72, # 3 p. 782 - 786
反应条件
1.1: H2SO4 1.2: pyridine / ethanol 2.1: triethylamine / dimethylformamide View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 5, # 12 p. 1915 - 1923
反应条件
1.1: H2SO4 1.2: pyridine / ethanol 2.1: triethylamine / dimethylformamide View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 5, # 12 p. 1915 - 1923
反应条件
1: 70 percent / Cu(II) 2: 98 percent / Et3N / dimethylformamide / 0.5 h / 60 °C View Scheme
参考文献
Synthetic Communications, , vol. 20, # 15 p. 2235 - 2249
反应条件
sodium hydroxide in 1,4-dioxane
参考文献
Justus Liebigs Annalen der Chemie, , vol. 716, p. 175 - 185
