2-溴-6-硝基苯甲酸甲酯合成路线 （共 3 条）
反应条件
in N,N-dimethyl-formamide T=0 - 20°C; 14 h;
参考文献
NOVARTIS AG; NOVARTIS PHARMA GmbH
Patent: WO2006/21454 A2, 2006 ;
Location in patent: Page/Page column 80; 81 ;
WO 2006/021454 A2
反应条件
caesium carbonate in methanol; N,N-dimethyl-formamide T=0 - 20°C; 14 h;
参考文献
Glossop, Steve C.
Synthesis, 2007 , # 7 p. 981 - 983
反应条件
1: 40 percent / KMnO4; Na2CO3 / H2O / 18 h / 100 °C 2: 100 percent / Cs2CO3 / methanol; dimethylformamide / 14 h / 0 - 20 °C View Scheme
参考文献
Hewson, Alan T.; Hughes, Kevin; Richardson, Steward K.; Sharpe, David A.; Wadsworth, Alan H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 6 p. 1565 - 1569
